Laboratory Procedures for Surveillance |
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LPS-001 |
Laboratory Procedure for the Determination of Benzene in Beverages |
June 5, 2006 |
LPS-002 |
Determination of Benzene in Soft Drinks and Other Beverages by Isotope Dilution Headspace Gas Chromatography/Mass Spectrometry |
November 22, 2007 |
LPS-003 |
The Determination of Acrylamide in Foods by LC-ESI-MS-MS |
January 8, 2008 |
LPS-004 |
Determination of Bisphenol A in Liquid Infant Formula by Solid Phase Extraction with Acetic Anhydride Derivatization and Gas Chromatography-Mass Spectrometry |
August, 2008 |
LPS-005 |
Determination of Melamine in Various Milk-Containing Products |
November, 2008 |
Official Methods |
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FO-1 |
Determination of protein rating |
October 15, 1981 |
FO-2 |
Determination of volatile acidity of wine, cider and champagne cider |
October 15, 1981 |
FO-3 |
Determination of carbon dioxide in baking powder |
October 15, 1981 |
FO-4 |
Determination of arsenic in food colours |
October 15, 1981 |
FO-5 |
Determination of lead in food colours |
October 15, 1981 |
FO-6 |
Determination of higher aromatic hydrocarbons or tarry materials in carbon black and charcoal |
October 15, 1981 |
FO-7 |
Determination of dye content of synthetic food colours |
March 15, 1984 |
FO-8 |
Determination of water insoluble matter in synthetic food colours |
March 15, 1984 |
FO-9 |
Determination of combined ether extracts in synthetic food colours |
March 15, 1984 |
FO-10 |
Determination of subsidiary dyes in synthetic food colours |
March 15, 1984 |
FO-11 |
Determination of intermediates in synthetic food colours |
March 15, 1984 |
FO-12 |
Determination of volatile matter in Citrus Red No. 2 |
March 15, 1984 |
FO-13 |
Determination of sulphated ash in Citrus Red No. 2 |
March 15, 1984 |
FO-14 |
Determination of water soluble matter in Citrus Red No. 2 |
March 15, 1984 |
FO-15 |
Determination of carbon tetrachloride insoluble matter in Citrus Red No. 2 |
March 15, 1984 |
FO-16 |
Determination of tocopherol in milk fat or butter fat |
October 15, 1981 |
FO-17 |
Extraction of soluble substances from vanilla beans |
September 15, 1989 |
FO-18 |
Determination of drained tomato solids |
October 15, 1981 |
FO-19 |
Determination of tomato solids |
October 15, 1981 |
FO-20 |
Determination of drained solids of beans with pork or beans and pork and beans or vegetarian beans |
October 15, 1981 |
FO-21 |
Determination of amino acids in grapefruit juice and orange juice |
October 15, 1981 |
FO-22 |
Determination of potassium in grapefruit juice and orange juice |
October 15, 1981 |
FO-23 |
Determination of absorbance value for total polyphenolics in grapefruit juice and orange juice |
October 15, 1981 |
FO-24 |
Determination of Brix reading for grapefruit juice and orange juice |
October 15, 1981 |
FO-25 |
Determination of acid in grapefruit juice or orange juice |
October 15, 1981 |
FO-26 |
Determination of soluble solids in lemon juice, lime juice or lime fruit juice |
October 15, 1981 |
FO-27 |
Determination of acid in lemon juice, lime juice or lime fruit juice |
October 15, 1981 |
FO-28 |
Determination of starch in gluten flour |
October 15, 1981 |
FO-29 |
Determination of moisture in grain |
October 15, 1981 |
FO-30 |
Determination of ash in grain |
October 15, 1981 |
FO-31 |
Determination of degree of fineness of grain |
October 15, 1981 |
FO-32 |
Determination of fillers, binders and dextrose equivalent |
October 15, 1981 |
FO-33 |
Determination of fat in meat and simulated meat products |
October 15, 1981 |
FO-34 |
Determination of ash in edible bone meal or edible bone flour |
October 15, 1981 |
FO-35 |
Determination of ash-free solids in gelatin |
October 15, 1981 |
FO-36 |
Determination of wiener content of meat specialties |
October 15, 1981 |
FO-37 |
Determination of water-soluble extractive in tea |
October 15, 1981 |
FO-38 |
Determination of salt in smoked fish |
March 15, 1985 |
FO-39 |
Determination of meat in boneless poultry |
October 15, 1981 |
FO-40 |
Determination of vinyl chloride in food |
October 15, 1981 |
FO-41 |
Determination of acrylonitrile in food |
February 16, 1982 |
FO-42 |
Determination of bioavailability of iron |
December 15, 1982 |
HPB Methods |
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HPB-FC-1 |
Determination of patulin by TLC |
July 1981 |
HPB-FC-2 |
Determination of docosenoic acid in fats and oil by GLC |
November 1981 |
HPB-FC-3 |
The determination of brominated vegetable oils in citrus-flavoured or spruce-flavoured beverages |
November 1981 |
HPB-FC-4 |
Determination of fluoride in food by micro-diffusion using a fluoride-specific electrode |
December 1981 |
HPB-FC-5 |
Determination of arsenic and selenium in foods (formerly LPFC-115) |
May 1982 |
HPB-FC-6 |
Determination of N-nitrosodimethylamine in beer at the lower parts per billion level by a GLC-thermal energy analyzer technique |
February 1982 |
HPB-FC-7 |
High performance liquid chromatographic determination of seven antioxidants in oil and lard (formerly LPFC-104) |
April 1982 |
HPB-FC-8 |
Determination of N-nitrosodimethylamine in non-fat dry milk |
January 1984 |
HPB-FC-9 |
Determination of tin in canned foods (formerly LPFC-112) |
June 1984 |
HPB-FC-10 |
Determination of ethyl carbamate in table wine, sherry, liquors and liqueurs |
April 1986 |
HPB-FC-11 |
Liquid chromatographic determination of domoic acid in mussels using the AOAC paralytic shellfish poison extraction procedure (formerly LPFC-151) |
March 1989 |
HPB-FC-12 |
Rapid gravimetric method for analysis of water-soluble and insoluble dietary fibre (formerly LPFC-142) |
January 1992 |
HPB-FC-13 |
Liquid chromatographic determination of nine antioxidants in butter oil |
October 1992 |
HPB-FC-14 |
High pressure liquid chromatographic determination of Aflatoxins in peanut butter and other commodities (formerly LPFC-124) |
June 1993 |
Laboratory Procedures |
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LPFC-100 |
Determination of monosodium glutamate in foods by GLC as trimethylsilyl derivative |
September 1978 |
LPFC-101 |
Direct analysis of carbofuran and two non-conjugated metabolites in foods by high-pressure liquid chromatography with UV absorption detection |
April 1978 |
LPFC-102 |
Determination of saccharin, sodium benzoate and caffeine in carbonated beverages by HPLC |
April 1980 |
LPFC-103 |
Determination of parabenz in beverages by GLC |
April 1979 |
LPFC-105 |
Determination of sorbic acid in fish |
November 1979 |
LPFC-106 |
Determination of ethylenediaminetetraacetic acids (EDTA) in fish |
November 1979 |
LPFC-107 |
Determination of ethoxylated mono- and diglycerides in bread |
November 1979 |
LPFC-108 |
Determination of barban in wheat products |
April 1980 |
LPFC-109 |
Comparison of liquid and gas chromatography for the determination of bromoxynil octanoate and benzoylprop-ethyl in wheat products |
May 1980 |
LPFC-110 |
Determination of lead and cadmium in foods by atomic absorption spectrophotometry |
August 1980 |
LPFC-111 |
Determination of ethoxyquin in spices |
October 1980 |
LPFC-114 |
Rapid screening determination of lead in canned milk and infant formulas using graphite-furnace atomic absorption spectrometry |
November 1980 |
LPFC-116 |
Rapid determination of lead and cadmium in foods using graphite-furnace atomic absorption spectrometry |
April 1981 |
LPFC-117 |
Determination of deoxynivalenol (vomitoxin, DON) in wheat and other grains by gas chromatography with electron capture and mass spectrometric detection |
January 1982 |
LPFC-118 |
Determination of metribuzin and its metabolites |
March 1982 |
LPFC-119 |
Determination of triforine in fruit |
March 1982 |
LPFC-120 |
Determination of Ergot alkaloids in wheat flour, rye flour and triticale flour |
July 1982 |
LPFC-121 |
A rapid method for the simultaneous analysis of diquat and paraquat in potatoes |
December 1982 |
LPFC-122 |
Determination of total lipids in foods |
April 1983 |
LPFC-123 |
Determination of deoxynivalenol (vomitoxin, DON) in wheat flour by gas chromatography with electron capture and mass spectrometric detection |
May 1983 |
LPFC-125 |
A rapid method for the determination of sodium and potassium |
June 1983 |
LPFC-126 |
Colorimetric determination of nitrate and nitrite in foods |
December 1983 |
LPFC-127 |
Screening test for the detection of sulphur dioxide in food products |
April 1984 |
LPFC-128 |
Determination of sucrose diacetate hexaisobutyrate (SAIB) in soft drinks |
April 1984 |
LPFC-129 |
Determination of egg-yolk solids in alimentary paste (formerly FA-1) |
October 1984 Amended June 1985 |
LPFC-130 |
Modified babcock method for fat in ground meat using paley bottles (formerly FA-33) |
October 1984 |
LPFC-131 |
Method for moisture in meat products (formerly FA-35) |
October 1984 |
LPFC-132 |
Determination of the percentage nuts in mixed nuts or a mixture of nuts (formerly FA-80, may be modified) |
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LPFC-133 |
Determination of methyl bromide in foods |
October 1984 |
LPFC-134 |
Determination of ethylene dibromide and other fumigants in foods |
November 1984 |
LPFC-135 |
Enzymatic determination of polyunsaturated fatty acids (PUFA) |
November 1984 |
LPFC-136 |
Determination of ethylene chlorohydrin in spices |
March 1985 |
LPFC-137 |
Sample preparation by dry ashing for the determination of various elements by flame atomic absorption spectroscopy |
April 1985 |
LPFC-138 |
Determination of nivalenol and deoxunivalenol (vomitoxin, DON) in cereals by gas chromatography with electron capture detection |
June 1985 Amended November 1989 |
LPFC-139 |
High performance liquid chromatographic determination of seven antioxidants in dry foods, mayonnaise and salad dressings |
December 1985 |
LPFC-140 |
Graphite-furnace atomic absorption spectrometric determination of lead and cadmium in foods after nitric-perchloric acid digestion and coprecipitation with ammonium pyrrolidine dithiocarbamate |
December 1985 |
LPFC-141 |
Graphite-furnace atomic absorption spectrometric determination of arsenic in foods after wet-dry ash and coprecipitation with ammonium pyrrolidine dithocarbamate |
February 1986 Amended January 1987 |
LPFC-143 |
Determination of diethylene glycol in wines by capillary gas chromatography |
June 1986 |
LPFC-144 |
Determination of nivalenol, deoxynivalenol (vomitoxin, DON), T-2 toxin, HT-2 toxin and diacetoxyscirpenol in cereals by gas chromatography with electron capture detection |
August 1986 |
LPFC-145 |
Gas chromatographic determination of polysaccharide gums in foods after hydrolysis and derivatization |
December 1986 |
LPFC-146 |
HPLC analysis of diquat and paraquat in potatoes |
January 1987 |
LPFC-147 |
An improved method for the determination of 1,1- dimethylhydrazine in apple and cherry products |
August 1987 |
LPFC-148 |
The determination of naptalam and its metabolite in foods as 1-naphthylamine using HPLC and oxidative electrochemical detection |
October 1987 |
LPFC-149 |
Determination of polycyclic aromatic hydrocarbons in foods by HPLC with fluorescence detection |
August 1987 |
LPFC-150 |
Determination of zearalenone and a- and b-zearalenols in milk by liquid chromatography with fluorescence detection |
December 1987 |
LPFC-152 |
Determination of fluazifop-butyl and fluazifop acid in soybeans and soybean oil using liquid chromatography with oxidative electrochemical detection |
July 1988 |
LPFC-153 |
Determination of alachlor and its 2,6-diethylaniline-containing metabolites in corn, soybeans and potatoes as heptafluorobutyryl-2,6-diethylaniline |
September 1988 |
LPFC-154 |
Determination of ergot alkaloids in wheat, rye and triticale flours, breads and bran |
December 1988 |
LPFC-155 |
Determination of nivalenol, deoxynivalenol (vomitoxin, DON), T-2 toxin, HT-2 toxin, 15-monacetoxyscirpenol and diacetoxyscirpenol in wheat and soybean by gas chromatography with electron capture detection |
July 1989 |
LPFC-156 |
Extraction and cleanup procedure for polychlorinated dioxins and furans in foods |
November 1989 |
LPFC-157 |
Determination of ochratoxin A in meat by high performance liquid chromatography with fluorometric detection |
November 1989 Amended December 1989 |
LPFC-158 |
Determination of sulfite in foods by liquid chromatography with amperometric detection |
February 1990 |
LPFC-159 |
Determination of ethylenethourea (ETU) in fruit juices |
May 1991 |
LPFC-160 |
Hydride generation atomic absorption spectrometric determination of selenium in foods |
December 1990 Amended March 1991 |
LPFC-161 |
Determination of fumonisins B1 and B2 in corn and corn meal by high performance liquid chromatography with fluorometric detection |
May 1991 Amended June 1991 |
LPFC-162 |
Sequential method for rapid determination of total dietary fibre |
June 1992 |
LPFC-163 |
Determination of methyl carbamate and ethyl carbamate in alcoholic beverages and other fermented foods |
May 1993 |
LPFC-164 |
Application of solid-phase microextraction to the headspace gas chromatographic analysis of halogenated volatiles in selected foods |
October 1993 Amended December 1993 |
LPFC-165 |
Graphite-furnace atomic absorption spectrometric determination of total aluminum, copper, manganese, molybdenum and tin in infant formulas and evaporated milks |
November 1994 |
LPFC-166 |
On-line steam distillation - purge and trap analysis of halogenated non-volatile contaminants in foods |
March 1995 |
LPFC-167 |
Liquid chromatographic determination of okadaic acid and dinophysistoxin-1 in shellfish after derivatization with 9-chloromethylanthracene |
June 1995 |
LPFC-200 |
The fluorometric determination of vitamin A in dairy products |
December 1986 |